Preparation of gold-palladium modified boron-doped diamond electrode and its preliminary test for oxygen sensors
At a Glance
Section titled āAt a Glanceā| Metadata | Details |
|---|---|
| Publication Date | 2018-01-01 |
| Journal | AIP conference proceedings |
| Authors | Muhammad S. P. Luhur, Tribidasari A. Ivandini, Munawar Khalil |
| Institutions | University of Indonesia |
| Citations | 4 |
Abstract
Section titled āAbstractāCore shell Au@Pd nanoparticles modified at boron-doped diamond (AuPd-BDD) electrodes were successfully prepared. Pd shell was formed at Au nanoparticles (AuNP) by the reduction reaction of H2PdCl4 to produce purple Au@Pd nanoparticles. The characterization performed using UV-Visible spectrophotometer showed the maximum wavelength at 523 nm, which decreased with the formation of Pd shell. The AuPd was then deposited on N-BDD surfaces and characterized using scanning electron microscopy (SEM) and X-Ray photoelectron spectroscopy (XPS). The modified electrode was used to determine the oxygen dissolved in phosphate buffer solution (PBS) by using cyclic voltammetry technique. Comparison between voltammograms of AuPd-N-BDD and AuNP-N-BDD indicated that the deposition of Au@Pd nanoparticles on N-BDD was successfully performed.