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Sample cell for studying liquid interfaces with anin situelectric field using X-ray reflectivity and application to clay particles at oil–oil interfaces

MetadataDetails
Publication Date2018-04-24
JournalJournal of Synchrotron Radiation
AuthorsSimon R. Larsen, Marie Hansteen, Barbara Pacáková, Keld Theodor, Thomas Arnold
InstitutionsNorwegian University of Science and Technology, Diamond Light Source
Citations2

Commissioning results of a liquid sample cell for X-ray reflectivity studies with an in situ applied electrical field are presented. The cell consists of a Plexiglas container with lateral Kapton windows for air-liquid and liquid-liquid interface studies, and was constructed with grooves to accept plate electrodes on the walls parallel to the direction of the beam. Both copper and ITO plate electrodes have been used, the latter being useful for simultaneous optical studies. Commissioning tests were made at the I07 beamline of the Diamond Light Source.