Simulation-Based Development of a New Cylindrical-Cavity Microwave-Plasma Reactor for Diamond-Film Synthesis
At a Glance
Section titled āAt a Glanceā| Metadata | Details |
|---|---|
| Publication Date | 2019-06-24 |
| Journal | Crystals |
| Authors | Qijun Wang, Gai Wu, Sheng Liu, Zhiyin Gan, Bo Yang |
| Institutions | Wuhan University, Huazhong University of Science and Technology |
| Citations | 21 |
Abstract
Section titled āAbstractāA 2.45 GHz microwave-plasma chemical-vapor deposition (MPCVD) reactor was designed and built in-house by collaborating with Guangdong TrueOne Semiconductor Technology Co., Ltd. A cylindrical cavity was designed as the deposition chamber and a circumferential coaxial-mode transformer located at the top of the cavity was adopted as the antenna. Two quartz-ring windows that were placed far away from the plasma and cooled by water-cooling cavity walls were used to affix the antenna to the cavity and act as a vacuum seal for the reactor, respectively. This design improved the sealing and protected the quartz windows. In addition, a numerical simulation was proposed to predict the electric-field and plasma-density distributions in the cavity. Based on the simulation results, a microwave-plasma reactor with TM021 mode was built. The leak rate of this new reactor was tested to be as low as 1 Ć 10ā8 PaĀ·m3Ā·sā1, and the maximal microwave power was as high as 10 kW. Then, single-crystal diamond films were grown with the morphology and crystalline quality characterized by an optical microscope, atomic force microscope (AFM), Raman spectrometer, photoluminescence (PL) spectrometer, and high-resolution X-ray diffractometer. It was shown that the newly developed MPCVD reactor can produce diamond films with high quality and purity.
Tech Support
Section titled āTech SupportāOriginal Source
Section titled āOriginal SourceāReferences
Section titled āReferencesā- 2008 - Diamond as an electronic material [Crossref]
- 2017 - Morphology of diamond layers grown on different facets of single crystal diamond substrates by a microwave plasma CVD in CH4-H2-N2 gas mixtures [Crossref]
- 2004 - Machining of electrically conductive CVD diamond tool blanks using EDM [Crossref]
- 2009 - Chemical vapour deposition synthetic diamond: materials, technology and applications [Crossref]
- 2006 - High rate homoepitaxial growth of diamond by microwave plasma CVD with nitrogen addition [Crossref]
- 2000 - A critical review of chemical vapor-deposited (CVD) diamond for electronic applications [Crossref]
- 2014 - High-rate homoepitaxial growth of CVD single-crystal diamond by dc arc plasma jet at blow-down (open cycle) mode [Crossref]
- 2012 - Fabrication and characterizations of large homoepitaxial single-crystal diamond grown by DC arc plasma jet CVD [Crossref]
- 2013 - The effect of deposition parameters on the morphology of micron diamond powders synthesized by HFCVD method [Crossref]
- 2016 - Synthesis and characterization of microcrystalline diamond to ultrananocrystalline diamond films via Hot Filament Chemical Vapor Deposition for scaling to large area applications [Crossref]