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Investigation of NV(−) centers and crystallite interfaces in synthetic single-crystal and polycrystalline nanodiamonds by optical fluorescence and microwave spectroscopy

MetadataDetails
Publication Date2018-02-01
JournalJournal of Optical Technology
AuthorsV. Yu. Osipov, N. M. Romanov, Kirill Bogdanov, François Treussart, Christian Jentgens
InstitutionsPeter the Great St. Petersburg Polytechnic University, Columbus NanoWorks (United States)
Citations6

Three types of diamond nanoparticles with sizes from 5 to 1000 nm have been investigated, whose crystal lattices include nitrogen-vacancy (NV) centers: detonation nanodiamonds (DNDs), dynamic-synthesis polycrystalline diamonds, and static-synthesis single-crystal diamonds. The electron paramagnetic resonance spectra have been investigated, along with the luminescence and IR absorption spectra of these materials. The DND concentration of NV(−) centers is 2.7 ppm and is highest for particles in the size range up to 7 nm. The concentration of NV(−) centers in polycrystalline diamonds is an order of magnitude less and depends on the average size of the polycrystalline particles, reaching a maximum at 180 nm in the average size range. The luminescence is brightest in 100-nm particles of synthetic Ib diamonds subjected to high-energy-electron irradiation and annealing. The latter with an NV(−) concentration of around 4 ppm can be used as fluorescent markers at the nanolevel.