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First Electroanalytical Methodology for the Determination of Hordenine in Dietary Supplements using a Boron‐doped Diamond Electrode

MetadataDetails
Publication Date2019-07-22
JournalElectroanalysis
AuthorsShabnam Allahverdiyeva, Ertuğrul Keskin, Pınar Talay Pınar, Yavuz Yardım, Zühre Şentürk
InstitutionsAdıyaman University, Van Yüzüncü Yıl Üniversitesi
Citations12

Abstract The present work describes the first electrochemical investigation and a simple, rapid and modification‐free electroanalytical methodology for quantification of hordenine (a potent phenylethylamine alkaloid) using a boron‐doped diamond electrode. At optimized square‐wave voltammetric parameters, the observed oxidation peak current in 0.1 M HClO 4 at +1.33 V (vs. Ag/AgCl) increased linearly from 5.0 to 100 μg mL −1 (3.0×10 −5 -6.1×10 −4 M), with detection limit of 1.3 μg mL −1 (7.8×10 −6 M). The applicability of the developed method was tested with the determination of hordenine in the commercial dietary supplement formulations.

  1. 2003 - Dietary Supplements of Plant Origin