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Diamond Field-Effect Transistors With V2O5-Induced Transfer Doping - Scaling to 50-nm Gate Length

MetadataDetails
Publication Date2020-05-06
JournalIEEE Transactions on Electron Devices
AuthorsKevin G. Crawford, James Weil, Pankaj B. Shah, Dmitry Ruzmetov, Mahesh R. Neupane
InstitutionsDEVCOM Army Research Laboratory
Citations28
AnalysisFull AI Review Included

This research details the successful fabrication and characterization of highly scaled hydrogen-terminated (H-terminated) diamond Field-Effect Transistors (FETs) utilizing Vanadium Pentoxide (V2O5) for robust surface transfer doping.

  • Record Performance: Devices achieved a peak drain current (Id,peak) of approximately 700 mA/mm and a peak transconductance (gm,peak) of 153 mS/mm, among the highest reported for diamond Metal Semiconductor FETs (MESFETs).
  • Critical Scaling: The gate length (Lg) was successfully scaled down to 50 nm, demonstrating the potential for improved performance through dimensional reduction.
  • Robust Doping Mechanism: V2O5, a high electron affinity transition metal oxide, was used as a stable surface acceptor, inducing a 2-D hole gas (2DHG) and improving device stability compared to volatile atmospheric adsorbents.
  • Inverse Scaling Observed: Peak output current and transconductance scaled inversely with gate length, confirming expected performance gains from scaling.
  • Channel Stability: Repeat measurements over 17 iterations showed high stability, with a standard deviation of only 3.1 mA/mm for the 200 nm device.
  • Material Improvement: Sheet resistance of the H-terminated diamond surface was reduced from 14.2 kΩ/square to 6.8 kΩ/square after V2O5 deposition.
  • Limitation Identified: Short channel effects, including Drain-Induced Barrier Lowering (DIBL) and gate instability (hot carrier injection), limit OFF-state performance at the smallest dimensions.
ParameterValueUnitContext
Peak Drain Current (Id,peak)~700mA/mm50 nm Lg, Vds = -10 V
Peak Transconductance (gm,peak)153mS/mm50 nm Lg, Vds = -4 V
Minimum Gate Length (Lg)50nmScaled device dimension
ON-Resistance (RON)6Ω.mm50 nm Lg, Vgs = -3 V
Sheet Resistance (Rsheet) Post-V2O56.8kΩ/squareVDP measurement
Sheet Resistance (Rsheet) Pre-V2O514.2kΩ/squareVDP measurement
Effective Mobility (”eff) (Estimated)23.5cm2 V-1 s-1Calculated using 400 nm Lg C-V data
Sheet Hole Density (p) (Estimated)3.9 x 1013cm-2Calculated using Rsheet
Maximum Gate Capacitance (Cg)1.15”F/cm2400 nm Lg, Vgs = -3 V
V2O5 Film Thickness40nmEncapsulation layer
V2O5 Deposition Anneal Temperature350°CIn situ anneal prior to V2O5 deposition
Gate Leakage (Ig) at Id,peak~1”A/mm50 nm Lg
Diamond Band-Gap5.47eVIntrinsic material property
Diamond Thermal Conductivity>20W cm-1 K-1Intrinsic material property
Diamond Breakdown Field10MV/cmIntrinsic material property
  1. Substrate Preparation: Single crystal diamond (100) was cleaned using H2SO4:NHO3 solution to remove metallic and organic contaminants, followed by hydrogen termination in a Chemical Vapor Deposition (CVD) reactor.
  2. Sacrificial Layer/Ohmic Contact: A 100 nm thick Au layer was thermally evaporated onto the substrate to serve as both a sacrificial layer and the basis for ohmic contacts.
  3. Device Isolation: Electrical isolation was achieved by patterning and etching the Au sacrificial layer between device regions using a KI2 solution. The exposed H-terminated diamond surface was then treated with O2 plasma to remove hydrogen termination in these isolation areas.
  4. Probe Pad Deposition: Ti/Au probe pads were written and deposited to overlap the Au ohmic metal, ensuring robust contact.
  5. Source-Drain Definition: The source-drain region was patterned and etched using a carefully controlled KI2 solution.
  6. Gate Stack Fabrication: Gate dimensions (50 nm to 800 nm) were defined using e-beam lithography, followed by the deposition of a metal gate-stack consisting of Al/Pt/Au (50/25/45 nm).
  7. Surface Annealing: A 350 °C in situ anneal was performed prior to the V2O5 deposition to drive off atmospheric molecules from the diamond surface, crucial for V2O5 work function stability.
  8. V2O5 Encapsulation: The substrate was encapsulated with 40 nm of V2O5 deposited via thermal evaporation to induce stable surface transfer doping.

The unique combination of diamond’s intrinsic properties (ultrawide band-gap, high thermal conductivity, high breakdown field) and the high-performance scaling demonstrated by this V2O5-doped FET technology targets several high-demand sectors:

  • Radio Frequency (RF) Electronics: High transconductance (153 mS/mm) and current density (700 mA/mm) make these devices ideal for high-frequency power amplifiers and switches in 5G/6G infrastructure and military communications.
  • High-Power Switching: Diamond’s 10 MV/cm breakdown field and superior thermal management (>20 W cm-1 K-1) enable next-generation power electronic devices (e.g., inverters, converters) operating at high voltages and temperatures.
  • Harsh Environment Electronics: The stability provided by the V2O5 encapsulation suggests suitability for electronics operating under extreme conditions (high temperature, high radiation).
  • Compact High-Density Circuits: The successful scaling to 50 nm gate lengths facilitates the integration of diamond FETs into dense, high-speed integrated circuits where small footprints are critical.
  • Diamond Metal Semiconductor FET (MESFET) Development: This work validates V2O5 as a robust alternative to traditional volatile dopants, accelerating the maturity of diamond MESFET technology.
View Original Abstract

We report on the fabrication and measurement of hydrogen-terminated diamond field-effect transistors (FETs) incorporating V2O5 as a surface acceptor material to induce transfer doping. Comparing a range of gate lengths down to 50 nm, we observe inversely scaling peak output current and transconductance. Devices exhibited a peak drain current of ~700 mA/mm and a peak transconductance of ~150 mS/mm, some of the highest reported thus far for a diamond metal semiconductor FET (MESFET). Reduced sheet resistance of the diamond surface after V2O5 deposition was verified by four probe measurement. These results show great potential for improvement of diamond FET devices through scaling of critical dimensions and adoption of robust transition metal oxides such as V2O5.