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Suppression of High Threshold Voltage for Boron-Doped Diamond MOSFETs

MetadataDetails
Publication Date2024-01-30
JournalIEEE Transactions on Electron Devices
AuthorsJiangwei Liu, Tokuyuki Teraji, Bo Da, Yasuo Koide
InstitutionsNational Institute for Materials Science
Citations6
AnalysisFull AI Review Included

This research focuses on suppressing the high threshold voltage (VTH) in Boron-doped Diamond (B-diamond) Metal-Oxide-Semiconductor Field-Effect Transistors (MOSFETs), a critical step toward realizing diamond complementary MOS (CMOS) circuits.

  • Core Achievement: Successfully suppressed VTH to a minimum of 0.8 V, significantly lower than previously reported values (up to 63.2 V).
  • Optimization Strategy: VTH reduction was achieved by carefully adjusting three key parameters: B-diamond epitaxial layer thickness (800 nm), boron doping concentration (1.36 x 1016 cm-3), and Al2O3 gate oxide thickness (45 nm).
  • Mechanism of Reduction: The combination of a thinner channel layer, lower dopant concentration, and a large absolute flat band voltage (|VFB| = 19.5 V) contributed to the dramatic decrease in VTH.
  • Device Performance: Fabricated devices demonstrated excellent switching characteristics, achieving on/off ratios greater than 106.
  • Output Current: Maximum drain currents (ID,max) ranged from -2.4 to -4.3 µA/mm, indicating a trade-off between low VTH and high output current density.
  • Interface Quality: The Al2O3/B-diamond heterojunction exhibited a Type II staggered band configuration with robust band offsets (VBO: 2.9 eV, CBO: 1.2 eV), resulting in low leakage current density (J) of approximately 10-8 A/cm2.
ParameterValueUnitContext
Lowest Threshold Voltage (VTH)0.8 ± 0.1VMOSFET-III
Maximum Drain Current (ID,max)-4.3µA/mmHighest measured value (MOSFET-II)
On/Off Ratio> 106N/AAll MOSFET types
Subthreshold Swing (SS)260mV/decLowest value (MOSFET-III)
B-Diamond Epitaxial Thickness800nmChannel layer
Boron Acceptor Concentration (NA)1.36 x 1016cm-3Deduced from C-2-V measurement
Gate Oxide Thickness (tox)45nmAl2O3 film (ALD)
Gate Oxide Dielectric Constant (k)8.0N/AUsed for theoretical Cox calculation
Surface Roughness (RMS)< 0.2nmB-diamond channel
Flat Band Voltage (VFB)19.5
Leakage Current Density (J)~10-8A/cm2At -19.0 V to 5.0 V
Valence Band Offset (VBO)2.9eVAl2O3/B-diamond heterojunction
Conduction Band Offset (CBO)1.2eVAl2O3/B-diamond heterojunction
Interface Trapped Charge Density (Dit)3.33 x 1012eV-1 cm-2Lowest value (MOSFET-III)
  1. B-Diamond Epitaxial Growth: A B-diamond epitaxial layer (800 nm thick) was grown on a well-polished Ib-type (100) diamond substrate using Microwave Plasma-Assisted Chemical Vapor Deposition (MPCVD).
  2. Substrate Cleaning and Preparation: The substrate was acid-cleaned using H2SO4 + HNO3 at 300 °C for 3 hours.
  3. Channel Surface Termination: The initial hydrogen-terminated surface was modified to an oxygen-terminated surface using a mixture acid solution (H2SO4 + HNO3) to form the stable B-diamond channel.
  4. Source/Drain Ohmic Contact Formation: Ti/Au (10/150 nm) electrodes were deposited via high-vacuum evaporation, followed by lift-off. Ohmic contact was achieved by Rapid Thermal Annealing (RTA) at 550 °C for 20 minutes.
  5. Gate Oxide Deposition: A 45 nm-thick Al2O3 film was deposited using Atomic Layer Deposition (ALD) at 200 °C, utilizing Al(CH3)3 and water vapor precursors.
  6. Gate Electrode Formation: Ti/Au (10/150 nm) gate electrodes were subsequently formed.
  7. Contact Window Etching: The Al2O3 layer covering the source/drain contacts was etched using Capacitively Coupled Plasma Reactive-Ion Etching (RIE). Process parameters included 100 W plasma power, 10 sccm CHF3 flow, and 40 sccm Ar flow.

The successful suppression of VTH in B-diamond MOSFETs addresses a major hurdle in diamond electronics, enabling new applications in high-performance and harsh-environment systems.

  • High-Temperature Electronics: The use of oxygen-terminated B-diamond channels provides superior thermal stability compared to traditional hydrogen-terminated diamond, making these devices ideal for high-temperature operation (e.g., downhole drilling, aerospace).
  • Diamond CMOS Logic Circuits: The achieved low VTH (0.8 V) is essential for designing energy-efficient diamond complementary MOS (CMOS) circuits, reducing the complexity and voltage requirements of the gate drive source.
  • High-Power Switching Devices: Diamond’s intrinsic properties (wide bandgap, high breakdown field) are leveraged for high-voltage power electronics and switching applications, although further efforts are needed to increase ID,max.
  • Radiation-Hardened Systems: Diamond’s inherent radiation hardness makes these MOSFETs suitable for use in nuclear, space, and defense applications where reliability under extreme conditions is paramount.
  • Integrated Circuits (ICs): The low VTH facilitates the integration of diamond transistors into complex digital and analog ICs, advancing the development of all-diamond integrated systems.
View Original Abstract

Suppression of high threshold voltage ( <inline-formula xmlns:mml=“http://www.w3.org/1998/Math/MathML” xmlns:xlink=“http://www.w3.org/1999/xlink”> <tex-math notation=“LaTeX”>${V} _{\text {TH}}$ </tex-math></inline-formula> ) for the boron-doped diamond (B-diamond) MOSFETs plays a key role to design the diamond complementary MOS circuits with low gate drive sources. The <inline-formula xmlns:mml=“http://www.w3.org/1998/Math/MathML” xmlns:xlink=“http://www.w3.org/1999/xlink”> <tex-math notation=“LaTeX”>${V} _{\text {TH}}$ </tex-math></inline-formula> can be further suppressed by adjusting B-diamond epitaxial layer thickness, boron doping concentration, and gate oxide thickness. Three MOSFETs with different device structures are fabricated on the same oxygen-terminated B-diamond channel. Thickness and acceptor concentration for the B-diamond epitaxial layer are approximately 800 nm and <inline-formula xmlns:mml=“http://www.w3.org/1998/Math/MathML” xmlns:xlink=“http://www.w3.org/1999/xlink”> <tex-math notation=“LaTeX”>$1.36\times 10^{{16}}$ </tex-math></inline-formula> cm−3, respectively. A 45 nm-thick Al2O3 is deposited as the gate oxide by an atomic layer deposition technique. Maximum drain currents and ON/OFF ratios for the B-diamond MOSFETs are in the range of <inline-formula xmlns:mml=“http://www.w3.org/1998/Math/MathML” xmlns:xlink=“http://www.w3.org/1999/xlink”> <tex-math notation=“LaTeX”>$-2.4\sim - 4.3,,\mu \text{A}$ </tex-math></inline-formula> /mm and greater than <inline-formula xmlns:mml=“http://www.w3.org/1998/Math/MathML” xmlns:xlink=“http://www.w3.org/1999/xlink”> <tex-math notation=“LaTeX”>$10^{{6}}$ </tex-math></inline-formula> , respectively. Their <inline-formula xmlns:mml=“http://www.w3.org/1998/Math/MathML” xmlns:xlink=“http://www.w3.org/1999/xlink”> <tex-math notation=“LaTeX”>${V} _{\text {TH}}$ </tex-math></inline-formula> values are lower than 3.4 V with the lowest one of 0.8 V.