Raman spectroscopy for studying the synthesis of conducting BC3 hetero-diamonds in diamond anvil cell under high temperature
At a Glance
Section titled āAt a Glanceā| Metadata | Details |
|---|---|
| Publication Date | 2020-05-01 |
| Journal | Journal of Physics Conference Series |
| Authors | A. A. Bykov, Pavel V. Zinin, Kamil M. Bulatov, Š. Š. Š¤ŠøŠ»Š¾Š½ŠµŠ½ŠŗŠ¾, Igor B. Kutuza |
| Institutions | Moscow Power Engineering Institute, Federal State Budgetary Institution of Science āScientific and Technological Center of Unique Instrumentationā of the Russian Academy of Sciences |
| Citations | 1 |
Abstract
Section titled āAbstractāAbstract A direct transformation of the sintered BC 3 phase to a novel diamond-like d -BC 3 phase was observed in a diamond anvil cell (DAC) at high temperature, 2500 K and high pressure, 22 GPa. For heating a specimen in a DAC a laser heating (LH) system combined with an acousto-optical filter and synchronized with a video camera was used. Combining the LH system with the acousto-optical filter allows measurement of the temperature distribution under infrared (1064 nm) LH of a specimen under high pressure in a DAC. The starting material with a composition BC 3 was obtained by sintering a powder of nanodiamonds with a powder of boron microparticles at 6.0 GPa during 150 s heating at 1200 Ā°C. The quenched BC 3 specimen was studied by the Raman spectroscopy.