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Simultaneous Determination of Young's Modulus and Density of Ultrathin Low‐k Films Using Surface Acoustic Waves

MetadataDetails
Publication Date2024-02-20
Journalphysica status solidi (a)
AuthorsLi Zhang, Xia Xiao, Jinsong Zhang, Zhuo Liu, Yiting Huang
InstitutionsTianjin University

The nondestructive testing (NDT) of mechanical properties in ultrathin low dielectric constant (low‐ k ) films is a major challenge in integrated circuit manufacturing. Young’s modulus and density are closely related parameters for low‐ k films. This study presents a method for NDT of Young’s modulus and density of porous low‐ k black diamond (SiOC:H, BD) films. A linear frequency modulation (LFM) surface acoustic wave (SAW) interdigital transducer (IDT) with a frequency range of 20-250 MHz is designed to generate SAW signals on the samples. The series of SAW waveforms obtained on the samples are processed to obtain experimental SAW dispersion curves across a broad frequency range. By comparing these experimental curves with theoretical dispersion curves, as well as their first‐order derivatives, Young’s modulus and density of porous low‐ k BD films with thicknesses of 100, 300, 500, and 1000 nm are characterized. To verify Young’s modulus measurements from the SAW method, a control experiment using nanoindentation is conducted. The results demonstrate that the SAW method can reduce the impact of the substrate and is independent of the film thickness. This study presents a highly accurate measuring method for simultaneous multiparameter evaluation of ultra‐thin low‐ k films.