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Optical Spin Initialization of Nitrogen Vacancy Centers in a 28Si-Enriched 6H-SiC Crystal for Quantum Technologies

MetadataDetails
Publication Date2024-04-01
JournalJournal of Experimental and Theoretical Physics Letters
AuthorsFadis F. Murzakhanov, Margarita A. Sadovnikova, G. V. Mamin, D. V. Shurtakova, E. N. Mokhov
InstitutionsKazan Federal University, Ioffe Institute
Citations5
AnalysisFull AI Review Included

This research demonstrates successful optical spin initialization and characterization of Nitrogen-Vacancy (NV-) centers in high-purity, 28Si-enriched 6H-SiC crystals, establishing them as promising solid-state qubits.

  • High Coherence Performance: Achieved exceptionally long electron spin relaxation times: T1 (longitudinal) = 1.3 ms and T2 (transverse) = 59 µs at 150 K (c || Bo orientation).
  • Isotope Engineering: The use of 28Si-enriched SiC (nuclear spin I = 0) minimizes electron-nuclear coupling noise, resulting in extremely narrow EPR absorption lines (450 kHz FWHM).
  • Optical Initialization: Effective spin alignment of the NV- ground state (Ms = 0) was achieved using nonresonant optical excitation at λ = 980 nm (3A → 3E transition).
  • High-Frequency Characterization: Three structurally nonequivalent axial NV- center types were identified and characterized using high-frequency (94 GHz, 3.4 T) pulsed Electron Paramagnetic Resonance (EPR).
  • Quantum Manipulation Potential: The combination of long relaxation times and narrow linewidths allows for highly selective excitation of resonant transitions, opening possibilities for complex quantum algorithms using optical, microwave, and radio-frequency pulse sequences.
ParameterValueUnitContext
Crystal Matrix6H-28SiCN/ASilicon isotope enriched (~99% 28Si, I=0)
Defect CenterNV-N/ANegatively charged Nitrogen-Vacancy (S=1)
Measurement Temperature150KOptimal for photoactive defect observation
EPR Frequency94GHzW band, pulsed EPR
Magnetic Field (Bo)3.4THigh-field regime (Zeeman interaction dominates)
Excitation Wavelength (λ)980nmNonresonant optical excitation
Transverse Relaxation Time (T2)59µsc
Longitudinal Relaxation Time (T1)1.3msc
EPR Linewidth (FWHM)450kHzExtremely narrow absorption lines
Electron Fluence (Irradiation)4 x 1018cm-2Used for vacancy defect formation
Fine Structure Splitting (D) (NVk1k2)1358 ± 2MHzAxial NV center type
Fine Structure Splitting (D) (NVhh)1331 ± 2MHzAxial NV center type
Fine Structure Splitting (D) (NVk2k1)1282 ± 2MHzAxial NV center type
Hyperfine Interaction (A)~1MHzWeak interaction with 14N (I=1) nuclei

The characterization relied on a sequence of material preparation steps followed by advanced pulsed EPR techniques:

  1. Crystal Growth: Bulk 6H-SiC crystals were grown via high-temperature physical vapor deposition (PVT) using a precursor enriched with the nonmagnetic 28Si isotope (I = 0) to achieve ~99% purity.
  2. Defect Induction: Crystals were irradiated with 2-MeV electrons at a fluence of 4 x 1018 cm-2 to create silicon and carbon vacancy defects.
  3. NV- Formation: Irradiated crystals were annealed in an argon atmosphere at T = 900 °C for 2 hours, optimizing the formation of stable NV- centers.
  4. Photoinduced EPR: Experiments were conducted using a commercial Bruker Elexsys E680 spectrometer (94 GHz, 3.4 T) at T = 150 K, coupled with a 980 nm continuous-wave laser for optical excitation and spin alignment.
  5. T2 Measurement: The transverse relaxation time was measured using the Hahn pulse sequence (π/2 - τ - π), detecting the electron spin echo integral intensity as a function of the delay time τ.
  6. T1 Measurement: The longitudinal relaxation time was measured using the “inversion-recovery” sequence (π - T - π/2 - τ - π), varying the time T between the inverting pulse and the detection sequence.

The demonstrated optical spin initialization and long coherence times in robust SiC matrices are critical for next-generation quantum technologies.

  • Solid-State Quantum Bits (Qubits): NV- centers in SiC are direct candidates for scalable solid-state qubits, offering a pathway to integrate quantum devices into existing semiconductor platforms.
  • Quantum Sensing: The high sensitivity of the NV- spin state to external fields enables the development of highly sensitive nanosensors for:
    • Magnetic field detection (magnetometry).
    • Temperature and pressure monitoring.
  • Quantum Cryptography: The ability to initialize and read out spin states optically supports the implementation of basic quantum cryptography protocols.
  • Near-Infrared Single-Photon Sources: The luminescence spectrum of SiC NV- centers (1.1-1.25 µm) falls within the O band, making them ideal single-photon sources for long-distance optical fiber information transmission.
  • Quantum Spintronics: The creation of a robust “photon-spin” interface allows for the fabrication of quantum spintronic elements, leveraging the spin alignment achieved through optical excitation.
View Original Abstract

High-spin defect centers in crystal matrices are used in quantum computing technologies, highly sensitive sensors, and single-photon sources. In this work, optically active nitrogen-vacancy color centers NV - in a 28 Si-enriched (nuclear spin $$I = 0$$ ) 6H- 28 SiC crystal have been studied using the photoinduced ( $$\lambda $$ = 980 nm) high-frequency (94 GHz, 3.4 T) pulsed electron paramagnetic resonance method at a temperature of $$T = 150{\kern 1pt} $$ K. Three structurally nonequivalent types of NV - centers with axial symmetry have been identified and their spectroscopic parameters have been determined. Long spin-lattice, $${{T}{1}} = 1.3{\kern 1pt} $$ ms, and spin-spin, $${{T}{2}} = 59{\kern 1pt} $$ μs, ensemble relaxation times of NV - centers with extremely narrow (450 kHz) absorption lines allow highly selective excitation of resonant transitions between sublevels $$({{m}_{I}})$$ caused by the weak hyperfine interaction $$(A \approx 1{\kern 1pt} $$ MHz) with 14 N $$(I = 1)$$ nuclei for the quantum manipulation of the electron spin magnetization.