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Rapid Growth of Polycrystalline Diamond Films by MPCVD at High Gas Pressure

MetadataDetails
Publication Date2015-01-01
AuthorsXueqi Zhou
InstitutionsAdvanced Diamond Technologies (United States)

Recent studies showed that increasing gas pressure and microwave power were effective methods to improve growth rate of diamond films by microwave plasma chemical vapor deposition( MPCVD). In this paper,polycrystalline diamond films were obtained at different methane concentrations in a newly developed cylindrical MPCVD reactor, using H2-CH4 as source gas. The gas pressure and input microwave power were fixed at 30 kPa and 5. 8 kW respectively. Surface morphologies,phases and qualities of the diamond films were measured by scanning electron microscopy,X-ray diffraction and Raman spectroscopy technologies. The results demonstrate that the growth rate of high quality diamond films deposited at high gas pressure raised from 7. 5μm/h to 27. 5μm/h when methane concentrations increased from 2. 5% to 5%.