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In-plane optical polarization and dynamic properties of the near-band-edge emission of an m-plane freestanding AlN substrate and a homoepitaxial film

MetadataDetails
Publication Date2019-10-07
JournalApplied Physics Letters
AuthorsShigefusa F. Chichibu, Kazunobu Kojima, K. Hazu, Y. Ishikawa, K. Furusawa
InstitutionsNorth Carolina State University, Tohoku University
Citations17

For accelerating the development of deep-ultraviolet light-emitting diodes based on high AlN mole fraction (x) AlxGa1-xN for sterilization, disinfection, and skin therapy applications, in-plane optical polarization and dynamic properties of the near-band edge (NBE) cathodoluminescence (CL) peak of a low threading dislocation density (<103 cmāˆ’2) m-plane freestanding AlN substrate and a homoepitaxial film are assessed. Consistent with the polarization selection rules, the electric field (E) component of the NBE emission was essentially polarized parallel to the c-axis (E∄c). Low-temperature CL spectra of the homoepitaxial film exhibited exciton fine structures: CL peaks at 6.0410 and 6.0279 eV, which were polarized E∄c and E perpendicular to the c-axis (E⊄c), respectively, are assigned as being due to the recombination of free A-excitons of irreducible representations Ī“1 and Ī“5. The hydrogenic binding energy of the Ī“1 A-exciton being 51 meV is verified. Detectable CL peaks under E∄c polarization at 6.0315 and 6.0212 eV are tentatively assigned as Ī“1-mixed Ī“5-exciton-polaritons. The concentration of multiple vacancies consisting of an Al-vacancy (VAl) and N-vacancies (VNs), namely, VAlVN2āˆ’3, in the substrate was estimated by the positron annihilation measurement to be 2-3 Ɨ 1016 cmāˆ’3, while that in the epilayer was lower than the detection limit (<1016 cmāˆ’3). The NBE CL lifetime of 28 ps of the epilayer subsurface at 300 K is likely limited by the recombination at carbon deep-acceptors on nitrogen sites (3 Ɨ 1017 cmāˆ’3) and/or VAlVN2āˆ’3 Shockley-Read-Hall nonradiative recombination centers (∼1 Ɨ 1016 cmāˆ’3) with hole capture coefficients of approximately 1Ɨ10āˆ’7 and 3Ɨ10āˆ’6 cm3 sāˆ’1, respectively.