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Optimal frequency measurements with quantum probes

MetadataDetails
Publication Date2021-04-01
Journalnpj Quantum Information
AuthorsSimon Schmitt, Tuvia Gefen, Daniel Louzon, Christian Osterkamp, Nicolas Staudenmaier
InstitutionsHebrew University of Jerusalem, Element Six (United Kingdom)
Citations18
AnalysisFull AI Review Included

This research outlines and experimentally validates optimal quantum strategies for frequency metrology using Nitrogen-Vacancy (NV) centers in diamond, achieving performance significantly beyond classical limits.

  • Optimal Discrimination: Demonstrated frequency discrimination of two signals separated by 2 kHz in a single 44 ”s measurement, achieving a speed factor of ten below the classical Fourier limit (1/T).
  • Near-Quantum Limit Estimation: Achieved a frequency estimation sensitivity of 1.6 ”Hz/Hz2 for a 1.7 ”T amplitude signal, which is within a factor of two of the theoretical Quantum Fisher Information (QFI) limit.
  • Optimal Control Protocol: The key innovation is the use of optimal coherent control (pi-pulses) synchronized to the signal, driving the sensor phase accumulation quadratically (t2) to maximize the angle between the states being discriminated.
  • Readout Comparison: Explicitly compared Ensemble Averaging (EA) and Single-Shot Readout (SSR) using a 13C ancilla qubit. SSR is shown to be advantageous (faster total measurement time) for long interaction periods (greater than 17 ”s) due to reduced overhead.
  • Foundational Impact: These results establish the fundamental limits and optimal protocols for discrimination and estimation problems critical to nanoscale Nuclear Magnetic Resonance (nano-NMR) spectroscopy.
ParameterValueUnitContext
Frequency Discrimination Time (Topt)44”sTime required to discriminate 2 kHz separation
Discrimination Speedup10xFactorImprovement over the classical Fourier limit
Signal Amplitude (B)1.7”TUsed during frequency estimation experiments
Frequency Estimation Sensitivity (Experimental)1.6”Hz/Hz2Achieved using Single-Shot Readout (SSR)
Quantum Fisher Information (QFI) Limit0.9”Hz/Hz2Theoretical limit for the 1.7 ”T signal (Eq. 8)
Bias Magnetic Field400GUsed to lift NV ground state degeneracy
Microwave Control Timing Resolution20psArbitrary Waveform Generator (AWG) specification
NV Phase Memory Time (T2*)~50”sTypical for 0.1% 13C diamond sample
13C Content (QND Sample)0.1%Diamond sample used for SSR experiments
Ancilla Readout Fidelity (NRR = 104)>99%Fidelity of the 13C nuclear spin readout
Ensemble Averaging Readout Overhead~1.5”sInitialization plus readout time per cycle
SSR Ancilla Readout Overhead (treadanc)~17”sTime required for repetitive mapping onto NV electron spin

The experiments utilize a single NV center in diamond as a quantum probe, employing precise microwave control and comparing two distinct readout strategies.

  • Quantum Probe Setup: A single NV center is used, optically initialized and read out via spin-dependent fluorescence detection using a confocal microscope. A 400 G magnetic field is applied along the NV axis to define the qubit states (0 and -1).
  • Optimal Coherent Control: The sensor is driven using sequences of pi-pulses (e.g., XY8-N) generated by a high-resolution AWG (20 ps timing). For optimal discrimination, pi-pulses are applied whenever the sign of the Hamiltonian difference (H1 - H2) changes, ensuring a continuous, quadratic (t2) accumulation of the phase difference (α).
  • Frequency Estimation Control: For optimal estimation, pi-pulses are applied at the signal antinodes (where the signal amplitude is maximal, corresponding to an initial phase Ξ = 0), maximizing the rate of phase accumulation.
  • Ensemble Averaging (EA): The standard method where the full sequence (initialization, sensing, optical readout) is repeated Nens times. Discrimination relies on reducing photon shot noise by increasing the total number of detected photons.
  • Single-Shot Readout (SSR) / Hybrid Strategy: The NV electron spin state is mapped onto a weakly coupled 13C nuclear spin (ancilla qubit). The ancilla state is then probed NRR times using a Quantum Non-Demolition (QND) measurement, allowing for high-fidelity readout (greater than 99% for NRR = 104).
  • Diamond Material: Experiments utilized ultrapure diamond, including samples with 0.1% 13C content for SSR, and isotopically enriched (99.999% 12C) layers for other tests. Samples were cleaned using a tri-acid mixture (H2SO4:HNO3:HClO4) at 130 °C.

The demonstrated optimal quantum metrology protocols are critical for applications requiring ultra-precise and fast frequency measurements, particularly in resource-limited environments.

  • Nanoscale NMR Spectroscopy: Enables high-resolution chemical analysis of extremely small sample volumes (e.g., single cells, single proteins) by maximizing the signal-to-noise ratio and minimizing measurement time.
  • Quantum Sensing and Metrology: Provides the fundamental protocols for constructing next-generation quantum sensors that operate at the theoretical limits of precision and speed.
  • Quantum System Characterization: Used for precise characterization of quantum systems, including measuring energy levels, estimating Hamiltonians, and determining coherence properties.
  • Improved Frequency Standards: The techniques for achieving near-quantum-limit frequency estimation can be applied to build more stable and accurate frequency standards.
  • Diagnostic and Screening Tools: The ability to perform rapid, high-fidelity frequency discrimination (e.g., “yes/no” questions about chemical presence) is valuable for fast diagnostic tests in medical or environmental monitoring.
  • Search for Dark Matter: The high sensitivity to small magnetic field oscillations makes these probes relevant for searches for exotic physics, such as axion-like dark matter.