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Development of 400°C operational relaxor ferroelectric based thin-film capacitor with exceptionally high stability

MetadataDetails
Publication Date2015-02-06
JournalThe Japan Society of Applied Physics
AuthorsSomu Kumaragurubaran

High-temperature operating electronic devices are indispensable for geothermal, automotive, space and aviation applications. SiC and diamond based transistors and diodes are capable of operating at 500C. In contrary, the capacitors can operate up to 175C only and are bulky too. Therefore, it is necessary to develop monolithic thin-film capacitors that can operate at least up to 400C. In the previous meeting, we demonstrated (1-x)[BaTiO3] xBi(Mg2/3Nb1/3)O3relaxor ferroelectric epitaxial thin-film capacitor that functions up to 400C [1]. However, the high-temperature stability of relative dielectric constant (r) was poor especially, at 25 - 100 C regime. Here, we show the exceptionally-high temperature stability of Ta doped BT-BMN compositionally engineered polycrystalline thin-film stacked capacitor. In the epitaxial capacitor, BT-BMN films were deposited using pulse laser deposition method. A significant out-diffusion of Bi was observed, in x-ray photoelectron spectroscopy analysis, on post-growth annealed BT-BMN surface. This caused the increase of dielectric loss and dielectric constant at high-temperatures that eventually lowered the temperature stability of the capacitor. To suppress the Bi out-diffusion Ta doped (max. 3 mol%) BT-BMN layer was introduced in the film at regular spacing. It significantly suppressed the Bi out-diffusion and improved the temperature stability of r and also the leakage current. However, the dielectric constant was dropped around room temperature. As a counter measure, we altered the composition ratio of BT and BMN film to shift the r peak-maximum towards low temperature region according to the results of bulk ceramics. Figure 1a depicts the compositionally engineered Ta doped BT-BMN film stack. Figure 1b shows the dielectric constant and dielectric loss as a function of temperature. Note that the dielectric constant exceeds 400 and the temperature stability is below 4% in 23-400C range at 50 kHz. [1] S. Kumaragurubaran et al. 75 th JSAP-Fall Annual Meetings, 18p-A9-2 (2014). 第62回応用物理学会春季学術講演会 講演予稿集 (2015 東海大学 湘南キャンパス) 13a-A21-8